Information card for entry 7250228

Structure parameters

• Formula: C34 H39 N3 Ni O6
• Calculated formula: C34 H39 N3 Ni O6
• Title of publication: Sequential Michael addition, cross-coupling and [3 + 2] cycloaddition reactions within the coordination sphere of chiral Ni(ii) Schiff base complexes derived from dehydroamino acids: pathways to the asymmetric synthesis of structurally diverse O-substituted serine and threonine analogs
• Authors of publication: Khachatryan, Emma A.; Sahakyan, Lusine Yu.; Tovmasyan, Anna S.; Melikyan, Gagik S.; Panosyan, Henrik A.; Mkrtchyan, Anna F.; Shibata, Norio; Malkov, Andrei V.; Saghyan, Ashot S.
• Journal of publication: RSC Advances
• Year of publication: 2025
• Journal volume: 15
• Journal issue: 14
• Pages of publication: 10558 - 10564
• a: 9.4105 ± 0.0001 Å
• b: 11.8727 ± 0.0001 Å
• c: 14.0699 ± 0.0002 Å
• α: 90°
• β: 95.565 ± 0.001°
• γ: 90°
• Cell volume: 1564.59 ± 0.03 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0229
• Residual factor for significantly intense reflections: 0.0226
• Weighted residual factors for significantly intense reflections: 0.0581
• Weighted residual factors for all reflections included in the refinement: 0.0583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No