Crystallography Open Database

Information card for entry 7700119

Preview

Coordinates	7700119.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C100 H88 Mg2 P4
Calculated formula	C100 H88 Mg2 P4
Title of publication	Reactivity of the carbodiphosphorane, (Ph<sub>3</sub>P)<sub>2</sub>C, towards main group metal alkyl compounds: coordination and cyclometalation.
Authors of publication	Quinlivan, Patrick J.; Shlian, Daniel G.; Amemiya, Erika; Parkin, Gerard
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	25
Pages of publication	9139 - 9151
a	14.655 ± 0.006 Å
b	10.248 ± 0.005 Å
c	26.929 ± 0.012 Å
α	90°
β	98.887 ± 0.007°
γ	90°
Cell volume	3996 ± 3 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1206
Residual factor for significantly intense reflections	0.0607
Weighted residual factors for significantly intense reflections	0.1423
Weighted residual factors for all reflections included in the refinement	0.1675
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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