Information card for entry 7700211

Structure parameters

• Formula: C66 H97 N4 O5 Si2 Sm Zn
• Calculated formula: C66 H97 N4 O5 Si2 Sm Zn
• Title of publication: Rare-earth/zinc heterometallic complexes containing both alkoxy-amino-bis(phenolato) and chiral salen ligands: synthesis and catalytic application for copolymerization of CO₂ with cyclohexene oxide.
• Authors of publication: Xu, Ruoyu; Hua, Linyan; Li, Xiang; Yao, Yingming; Leng, Xuebing; Chen, Yaofeng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 28
• Pages of publication: 10565 - 10573
• a: 10.3825 ± 0.0002 Å
• b: 26.0638 ± 0.0005 Å
• c: 15.2519 ± 0.0003 Å
• α: 90°
• β: 108.751 ± 0.0009°
• γ: 90°
• Cell volume: 3908.22 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0959
• Weighted residual factors for all reflections included in the refinement: 0.0966
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No