Information card for entry 7700249

Structure parameters

• Formula: C14 H33 Li N2 Si
• Calculated formula: C14 H33 Li N2 Si
• Title of publication: The smaller, the better? How the aggregate size affects the reactivity of (trimethylsilyl)methyllithium.
• Authors of publication: Knauer, Lena; Wattenberg, Jonathan; Kroesen, Ulrike; Strohmann, Carsten
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 30
• Pages of publication: 11285 - 11291
• a: 7.4127 ± 0.0003 Å
• b: 12.3217 ± 0.0005 Å
• c: 10.0582 ± 0.0004 Å
• α: 90°
• β: 105.694 ± 0.002°
• γ: 90°
• Cell volume: 884.44 ± 0.06 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0345
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0885
• Weighted residual factors for all reflections included in the refinement: 0.0898
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No