Information card for entry 7700270

Structure parameters

• Formula: C22 H50 B F6 N O2 Pb Si4
• Calculated formula: C22 H50 B F6 N O2 Pb Si4
• Title of publication: Aminofluoroalkoxide amido and boryloxo lead(ii) complexes.
• Authors of publication: Someşan, Adrian-Alexandru; Roisnel, Thierry; Dorcet, Vincent; Silvestru, Cristian; Sarazin, Yann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 27
• Pages of publication: 9944 - 9948
• a: 13.087 ± 0.0013 Å
• b: 9.0118 ± 0.0008 Å
• c: 29.884 ± 0.003 Å
• α: 90°
• β: 100.753 ± 0.004°
• γ: 90°
• Cell volume: 3462.6 ± 0.6 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.044
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0722
• Weighted residual factors for all reflections included in the refinement: 0.075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.25
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No