Information card for entry 7700297

Structure parameters

• Formula: C52 H94 Cl2 F2 N8 Si4
• Calculated formula: C52 H94 Cl2 F2 N8 Si4
• Title of publication: NHC-stabilized silyl-substituted silyliumylidene ions.
• Authors of publication: Frisch, Philipp; Inoue, Shigeyoshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 28
• Pages of publication: 10403 - 10406
• a: 11.0482 ± 0.0019 Å
• b: 17.171 ± 0.003 Å
• c: 21.066 ± 0.004 Å
• α: 66.805 ± 0.005°
• β: 74.978 ± 0.005°
• γ: 88.261 ± 0.006°
• Cell volume: 3536.2 ± 1.1 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0802
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1114
• Weighted residual factors for all reflections included in the refinement: 0.1207
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No