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Information card for entry 7700317
Preview
Coordinates | 7700317.cif |
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Original paper (by DOI) | HTML |
Formula | C25 H51 N4 Nd Si4 |
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Calculated formula | C25 H51 N4 Nd Si4 |
Title of publication | Synthesis and characterization of 2-t-butylimino-functionalized indolyl rare-earth metal amido complexes for the catalytic addition of terminal alkynes to carbodiimides: the dimeric complexes with the alkynide species in the μ-η<sup>1</sup>:η<sup>2</sup> bonding modes. |
Authors of publication | Feng, Zhijun; Huang, Zeming; Wang, Shaowu; Wei, Yun; Zhou, Shuangliu; Zhu, Xiancui |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 29 |
Pages of publication | 11094 - 11102 |
a | 18.3322 ± 0.0011 Å |
b | 11.726 ± 0.0007 Å |
c | 17.2138 ± 0.001 Å |
α | 90° |
β | 108.536 ± 0.001° |
γ | 90° |
Cell volume | 3508.4 ± 0.4 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293.15 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0369 |
Residual factor for significantly intense reflections | 0.0257 |
Weighted residual factors for significantly intense reflections | 0.0606 |
Weighted residual factors for all reflections included in the refinement | 0.0657 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7700317.html
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