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Information card for entry 7700367
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Coordinates | 7700367.cif |
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Original paper (by DOI) | HTML |
Formula | C46 H35 B F15 O4 P |
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Calculated formula | C46 H35 B F15 O4 P |
Title of publication | Carbon-carbon bond forming reactions of acetylenic esters and ketones within frustrated phosphane/borane Lewis pair frameworks. |
Authors of publication | Wang, Long; Li, Jun; Deng, Dongsheng; Daniliuc, Constantin G.; Mück-Lichtenfeld, Christian; Kehr, Gerald; Erker, Gerhard |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 31 |
Pages of publication | 11921 - 11926 |
a | 11.5331 ± 0.001 Å |
b | 22.0907 ± 0.0017 Å |
c | 19.0773 ± 0.0016 Å |
α | 90° |
β | 94.56 ± 0.005° |
γ | 90° |
Cell volume | 4845 ± 0.7 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1024 |
Residual factor for significantly intense reflections | 0.0631 |
Weighted residual factors for significantly intense reflections | 0.1584 |
Weighted residual factors for all reflections included in the refinement | 0.182 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.006 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7700367.html
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