Information card for entry 7700416

Structure parameters

• Formula: C32 H39 F6 N2 O4 Pd2 Sb
• Calculated formula: C32 H39 F6 N2 O4 Pd2 Sb
• Title of publication: Antimony(i) →Pd(ii) complexes with the (μ-Sb)Pd₂ coordination framework.
• Authors of publication: Kořenková, Monika; Hejda, Martin; Jirásko, Robert; Block, Theresa; Uhlík, Filip; Jambor, Roman; RůŽička, Aleš; Pöttgen, Rainer; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 31
• Pages of publication: 11912 - 11920
• a: 18.3001 ± 0.0013 Å
• b: 10.5868 ± 0.0006 Å
• c: 18.5561 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3595 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.1108
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for significantly intense reflections: 0.0745
• Weighted residual factors for all reflections included in the refinement: 0.0856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No