Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7700474
Preview
Coordinates | 7700474.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H36 F6 N P3 Ru |
---|---|
Calculated formula | C39 H36 F6 N P3 Ru |
Title of publication | Facile synthesis of 1,5-disubstituted tetrazoles by reacting a ruthenium acetylide complex with trimethylsilyl azide. |
Authors of publication | Chang, Chao-Wan; Cheng, Ming-Chuan; Lee, Gene-Hsiang; Peng, Shie-Ming |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 31 |
Pages of publication | 11732 - 11742 |
a | 10.803 ± 0.0003 Å |
b | 16.603 ± 0.0005 Å |
c | 20.3682 ± 0.0006 Å |
α | 87.6054 ± 0.0007° |
β | 88.2701 ± 0.0007° |
γ | 87.3777 ± 0.0007° |
Cell volume | 3644.81 ± 0.18 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0702 |
Residual factor for significantly intense reflections | 0.0556 |
Weighted residual factors for significantly intense reflections | 0.1174 |
Weighted residual factors for all reflections included in the refinement | 0.1264 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.1 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7700474.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.