Information card for entry 7700480

Structure parameters

• Formula: C24 H18 Cl N3 Ni O
• Calculated formula: C24 H18 Cl N3 Ni O
• Title of publication: Tridentate diarylamido-based pincer complexes of nickel and palladium: sidearm effects in the polymerization of norbornene.
• Authors of publication: You, Fen; Liu, Hui; Luo, Gen; Shi, Xiaochao
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 32
• Pages of publication: 12219 - 12227
• a: 9.18 ± 0.003 Å
• b: 9.941 ± 0.003 Å
• c: 11.212 ± 0.004 Å
• α: 90°
• β: 102.531 ± 0.003°
• γ: 90°
• Cell volume: 998.8 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0221
• Residual factor for significantly intense reflections: 0.0207
• Weighted residual factors for significantly intense reflections: 0.0496
• Weighted residual factors for all reflections included in the refinement: 0.0504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No