Information card for entry 7700512

Structure parameters

• Formula: C12 H15 I6 N2 O4 Re Te2
• Calculated formula: C12 H13 I6 N2 O4 Re Te2
• Title of publication: Ionic-liquid-based synthesis of tellurium-rhenium carbonyls with specific reaction control.
• Authors of publication: Wolf, Silke; Feldmann, Claus
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 41
• Pages of publication: 15521 - 15528
• a: 9.7094 ± 0.0019 Å
• b: 13.539 ± 0.003 Å
• c: 22.976 ± 0.006 Å
• α: 90°
• β: 108.62 ± 0.03°
• γ: 90°
• Cell volume: 2862.2 ± 1.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0411
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.093
• Weighted residual factors for all reflections included in the refinement: 0.096
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No