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Information card for entry 7700679
Preview
Coordinates | 7700679.cif |
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Original paper (by DOI) | HTML |
Formula | C32 H51 O2 P2 Pd Ru |
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Calculated formula | C32 H51 O2 P2 Pd Ru |
Title of publication | Synthesis, structural properties and reactivity of ruthenocene-based pincer Pd(ii) tetrahydroborate. |
Authors of publication | Safronov, Sergey V.; Gutsul, Evgenii I.; Golub, Igor E.; Dolgushin, Fedor M.; Nelubina, Yulia V.; Filippov, Oleg A.; Epstein, Lina M.; Peregudov, Alexander S.; Belkova, Natalia V.; Shubina, Elena S. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 33 |
Pages of publication | 12720 - 12729 |
a | 9.892 ± 0.0005 Å |
b | 12.0215 ± 0.0006 Å |
c | 15.1339 ± 0.0007 Å |
α | 109.11 ± 0.001° |
β | 105.389 ± 0.001° |
γ | 96.936 ± 0.001° |
Cell volume | 1596.37 ± 0.14 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0496 |
Residual factor for significantly intense reflections | 0.0352 |
Weighted residual factors for significantly intense reflections | 0.0697 |
Weighted residual factors for all reflections included in the refinement | 0.0764 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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