Information card for entry 7700746

Structure parameters

• Formula: C15 H15 B Cl F4 N6 O Pd
• Calculated formula: C15 H15 B Cl F4 N6 O Pd
• Title of publication: Synthesis and redox chemistry of Pd(ii) complexes of a pincer verdazyl ligand.
• Authors of publication: Sanz, Corey A.; Patrick, Brian O.; Hicks, Robin G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12674 - 12683
• a: 8.6741 ± 0.0004 Å
• b: 15.7852 ± 0.0008 Å
• c: 14.5177 ± 0.0007 Å
• α: 90°
• β: 100.721 ± 0.003°
• γ: 90°
• Cell volume: 1953.1 ± 0.16 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0901
• Weighted residual factors for all reflections included in the refinement: 0.0958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No