Information card for entry 7700772

Structure parameters

• Formula: C48.33 H57.33 F6 N2 O4.33 P3 Re
• Calculated formula: C46 H48 F6 N2 O2 P3 Re
• Title of publication: Steric influence of salicylaldehyde-based Schiff base ligands on the formation of trans-[Re(PR₃)₂(Schiff base)]⁺ complexes.
• Authors of publication: Baumeister, Jakob E.; Mitchell, Andrew W.; Kelley, Steven P.; Barnes, Charles L.; Jurisson, Silvia S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 34
• Pages of publication: 12943 - 12955
• a: 42.45 ± 0.004 Å
• b: 10.1296 ± 0.0009 Å
• c: 30.348 ± 0.003 Å
• α: 90°
• β: 130.284 ± 0.001°
• γ: 90°
• Cell volume: 9954.9 ± 1.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.026
• Residual factor for significantly intense reflections: 0.0196
• Weighted residual factors for significantly intense reflections: 0.0431
• Weighted residual factors for all reflections included in the refinement: 0.0452
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No