Information card for entry 7700789

Structure parameters

• Formula: C25.5 H14 B Cl F9 N2 O
• Calculated formula: C25.5 H14 B Cl F9 N2 O
• Title of publication: Reactions of hydrazones and hydrazides with Lewis acidic boranes.
• Authors of publication: Gazis, Theodore A.; Dasgupta, Ayan; Hill, Michael S.; Rawson, Jeremy M.; Wirth, Thomas; Melen, Rebecca L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12391 - 12395
• a: 25.9971 ± 0.001 Å
• b: 15.1972 ± 0.0006 Å
• c: 13.0295 ± 0.0004 Å
• α: 90°
• β: 94.668 ± 0.003°
• γ: 90°
• Cell volume: 5130.7 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for significantly intense reflections: 0.1681
• Weighted residual factors for all reflections included in the refinement: 0.179
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No