Information card for entry 7700872

Structure parameters

• Formula: C36 H51 N2 P3
• Calculated formula: C36 H51 N2 P3
• Title of publication: Oligomerization of phosphaalkynes mediated by bulky N-heterocyclic carbenes: avenues to novel phosphorus frameworks.
• Authors of publication: Liu, Liu Leo; Zhou, Jiliang; Kim, Youngsuk; Cao, Levy L.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 38
• Pages of publication: 14242 - 14245
• a: 14.69 ± 0.008 Å
• b: 12.143 ± 0.007 Å
• c: 19.672 ± 0.01 Å
• α: 90°
• β: 95.572 ± 0.012°
• γ: 90°
• Cell volume: 3493 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1415
• Weighted residual factors for all reflections included in the refinement: 0.1686
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No