Information card for entry 7700961

Structure parameters

• Formula: Ca9 Li6.28 Sn12.72
• Calculated formula: Ca9 Li6.284 Sn12.716
• Title of publication: Multifaceted Sn-Sn bonding in the solid state. Synthesis and structural characterization of four new Ca-Li-Sn compounds.
• Authors of publication: Ovchinnikov, Alexander; Bobev, Svilen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 38
• Pages of publication: 14398 - 14407
• a: 17.21 ± 0.002 Å
• b: 4.6081 ± 0.0006 Å
• c: 18.881 ± 0.002 Å
• α: 90°
• β: 107.81 ± 0.002°
• γ: 90°
• Cell volume: 1425.6 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 3
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0351
• Weighted residual factors for significantly intense reflections: 0.0732
• Weighted residual factors for all reflections included in the refinement: 0.0776
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No