Information card for entry 7701117

Structure parameters

• Formula: C22 H24 B2 F8 Fe N10
• Calculated formula: C22 H24 B2 F8 Fe N10
• Title of publication: Iron(ii) tetrafluoroborate complexes of new tetradentate C-scorpionates as catalysts for the oxidative cleavage of trans-stilbene with H₂O₂.
• Authors of publication: Wang, Denan; Gardinier, James R.; Lindeman, Sergey V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 38
• Pages of publication: 14478 - 14489
• a: 10.907 ± 0.0007 Å
• b: 11.7927 ± 0.0007 Å
• c: 12.8472 ± 0.0008 Å
• α: 68.952 ± 0.006°
• β: 84.954 ± 0.006°
• γ: 63.988 ± 0.007°
• Cell volume: 1381.2 ± 0.18 ų
• Cell temperature: 103.7 ± 0.1 K
• Ambient diffraction temperature: 103.7 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0572
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.1322
• Weighted residual factors for all reflections included in the refinement: 0.1428
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No