Information card for entry 7701211

Structure parameters

• Formula: C30 H51 As Fe N2 Si4
• Calculated formula: C30 H51 As Fe N2 Si4
• Title of publication: Magnetic anisotropy in trigonal planar Fe(ii) bis(trimethylsilyl)amido complexes of the type [Fe{N(SiMe₃)₂}₂L]-experiment and theory.
• Authors of publication: Bodenstein, Tilmann; Eichhöfer, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 41
• Pages of publication: 15699 - 15712
• a: 10.0844 ± 0.0005 Å
• b: 13.4794 ± 0.0006 Å
• c: 13.8294 ± 0.0007 Å
• α: 90.654 ± 0.004°
• β: 93.729 ± 0.004°
• γ: 91.626 ± 0.004°
• Cell volume: 1874.95 ± 0.16 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.084
• Weighted residual factors for all reflections included in the refinement: 0.0871
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No