Information card for entry 7701502

Structure parameters

• Formula: C35 H92 O3 Si12
• Calculated formula: C35 H92 O3 Si12
• Title of publication: Reactions of a tetrasilabicyclo[1.1.0]but-1(3)-ene with carbon tetrachloride and methanol.
• Authors of publication: Nukazawa, Takumi; Kosai, Tomoyuki; Honda, Shunya; Ishida, Shintaro; Iwamoto, Takeaki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 10874 - 10880
• a: 11.3627 ± 0.0005 Å
• b: 16.4034 ± 0.0008 Å
• c: 17.0141 ± 0.0008 Å
• α: 112.053 ± 0.001°
• β: 94.225 ± 0.001°
• γ: 109.529 ± 0.001°
• Cell volume: 2697.1 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0313
• Residual factor for significantly intense reflections: 0.0273
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0785
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No