Information card for entry 7701620

Structure parameters

• Formula: C34 H40 B N Si
• Calculated formula: C34 H40 B N Si
• Title of publication: Expansion of the scope of alkylboryl-bridged N →B-ladder boranes: new substituents and alternative substrates.
• Authors of publication: Pammer, Frank; Schepper, Jonas; Glöckler, Johannes; Sun, Yu; Orthaber, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 27
• Pages of publication: 10298 - 10312
• a: 12.8845 ± 0.0003 Å
• b: 11.7689 ± 0.0003 Å
• c: 20.7907 ± 0.0007 Å
• α: 90°
• β: 102.702 ± 0.003°
• γ: 90°
• Cell volume: 3075.47 ± 0.15 ų
• Cell temperature: 149.95 ± 0.1 K
• Ambient diffraction temperature: 149.95 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0678
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1152
• Weighted residual factors for all reflections included in the refinement: 0.1255
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No