Information card for entry 7701643

Structure parameters

• Formula: C18 H36 B Br N P
• Calculated formula: C18 H36 B Br N P
• Title of publication: Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes.
• Authors of publication: Ordyszewska, Anna; Szynkiewicz, Natalia; Perzanowski, Emil; Chojnacki, Jarosław; Wiśniewska, Aleksandra; Grubba, Rafał
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12482 - 12495
• a: 9.3592 ± 0.0003 Å
• b: 10.4885 ± 0.0004 Å
• c: 11.7596 ± 0.0004 Å
• α: 78.374 ± 0.003°
• β: 78.775 ± 0.003°
• γ: 64.478 ± 0.003°
• Cell volume: 1012.73 ± 0.07 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0308
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0748
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No