Crystallography Open Database

Information card for entry 7701648

Preview

Coordinates	7701648.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H34 B N P2
Calculated formula	C30 H34 B N P2
Title of publication	Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes.
Authors of publication	Ordyszewska, Anna; Szynkiewicz, Natalia; Perzanowski, Emil; Chojnacki, Jarosław; Wiśniewska, Aleksandra; Grubba, Rafał
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	33
Pages of publication	12482 - 12495
a	9.7043 ± 0.0006 Å
b	10.326 ± 0.0008 Å
c	14.6037 ± 0.0011 Å
α	106.292 ± 0.006°
β	95.312 ± 0.006°
γ	106.653 ± 0.006°
Cell volume	1321.69 ± 0.18 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1395
Residual factor for significantly intense reflections	0.0802
Weighted residual factors for significantly intense reflections	0.1964
Weighted residual factors for all reflections included in the refinement	0.2266
Goodness-of-fit parameter for all reflections included in the refinement	0.941
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7701648.html