Information card for entry 7701651

Structure parameters

• Formula: C22 H41 B P2
• Calculated formula: C22 H41 B P2
• Title of publication: Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes.
• Authors of publication: Ordyszewska, Anna; Szynkiewicz, Natalia; Perzanowski, Emil; Chojnacki, Jarosław; Wiśniewska, Aleksandra; Grubba, Rafał
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12482 - 12495
• a: 8.5349 ± 0.0004 Å
• b: 10.8909 ± 0.0006 Å
• c: 13.1235 ± 0.0007 Å
• α: 80.516 ± 0.004°
• β: 80.617 ± 0.004°
• γ: 81.687 ± 0.004°
• Cell volume: 1178.38 ± 0.11 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0398
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.095
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No