Information card for entry 7701659

Structure parameters

• Formula: C8 H24 N4 O62 Ru1.02 Sb W16.98
• Calculated formula: C8.0016 H27.6048 N3.9996 O61.9996 Ru1.02 Sb W16.98
• Title of publication: Reactions of [Ru(NO)Cl₅]^2- with pseudotrilacunary {XW₉O₃₃}^9- (X = As^III, Sb^III) anions.
• Authors of publication: Mukhacheva, Anna A.; Shmakova, Alexandra A.; Volchek, Victoria V.; Romanova, Tamara E.; Benassi, Enrico; Gushchin, Artem L.; Yanshole, Vadim; Sheven, Dmitri G.; Kompankov, Nikolay B.; Abramov, Pavel A.; Sokolov, Maxim N.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 42
• Pages of publication: 15989 - 15999
• a: 21.1706 ± 0.0014 Å
• b: 21.1706 ± 0.0014 Å
• c: 15.68 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6086.2 ± 1 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.0579
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No