Information card for entry 7701673

Structure parameters

• Formula: C52 H40 Cu1.5 Dy F36 N8 O16
• Calculated formula: C52 H40 Cu1.5 Dy F36 N8 O16
• Title of publication: Synthesis of a series of hetero-multi-spin Ln₂Cu₃ complexes based on a methyl-pyrazole nitronyl nitroxide radical with slow magnetic relaxation behaviors.
• Authors of publication: Shi, Jian Yun; Chen, Peng Yun; Wu, Ming Ze; Tian, Li; Liu, Zhong Yi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 25
• Pages of publication: 9187 - 9193
• a: 11.9061 ± 0.0002 Å
• b: 18.3248 ± 0.0005 Å
• c: 20.332 ± 0.0005 Å
• α: 94.322 ± 0.002°
• β: 92.4181 ± 0.0017°
• γ: 95.6122 ± 0.0019°
• Cell volume: 4396.66 ± 0.18 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0773
• Residual factor for significantly intense reflections: 0.0665
• Weighted residual factors for significantly intense reflections: 0.1664
• Weighted residual factors for all reflections included in the refinement: 0.1759
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No