Information card for entry 7701683

Structure parameters

• Formula: C53 H64 As2 Cl4 N2 O Zr
• Calculated formula: C53 H64 As2 Cl4 N2 O Zr
• Title of publication: Synthesis and structural characterization of arsinoamides - early transition metal (Zr and Hf) and main group metal (Al, In, Sn, and Pb) complexes.
• Authors of publication: Chen, Xiao; Gamer, Michael T.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 40
• Pages of publication: 15207 - 15211
• a: 12.3693 ± 0.0006 Å
• b: 16.8828 ± 0.0005 Å
• c: 25.026 ± 0.0011 Å
• α: 90°
• β: 102.369 ± 0.004°
• γ: 90°
• Cell volume: 5104.8 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1011
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.1107
• Weighted residual factors for all reflections included in the refinement: 0.1305
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No