Information card for entry 7701686

Structure parameters

• Formula: C52 H66 As2 Hf N4
• Calculated formula: C52 H66 As2 Hf N4
• Title of publication: Synthesis and structural characterization of arsinoamides - early transition metal (Zr and Hf) and main group metal (Al, In, Sn, and Pb) complexes.
• Authors of publication: Chen, Xiao; Gamer, Michael T.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 40
• Pages of publication: 15207 - 15211
• a: 9.3307 ± 0.0004 Å
• b: 13.5735 ± 0.0006 Å
• c: 19.6583 ± 0.0009 Å
• α: 95.723 ± 0.003°
• β: 96.008 ± 0.004°
• γ: 103.085 ± 0.004°
• Cell volume: 2392.11 ± 0.19 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0436
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0789
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No