Crystallography Open Database

Information card for entry 7701763

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Coordinates	7701763.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H83 N4 O Si4 Sm
Calculated formula	C47 H83 N4 O Si4 Sm
Title of publication	Mono- and bimetallic amidinate samarium complexes - synthesis, structure, and hydroamination catalysis.
Authors of publication	Kazeminejad, Neda; Münzfeld, Luca; Gamer, Michael T.; Roesky, Peter W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	23
Pages of publication	8153 - 8160
a	12.0107 ± 0.0007 Å
b	26.4912 ± 0.0018 Å
c	17.3028 ± 0.001 Å
α	90°
β	95.898 ± 0.005°
γ	90°
Cell volume	5476.2 ± 0.6 Å³
Cell temperature	210 K
Ambient diffraction temperature	210 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.071
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.0783
Weighted residual factors for all reflections included in the refinement	0.0836
Goodness-of-fit parameter for all reflections included in the refinement	0.857
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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