Molecular Squares, Coordination Polymers and Mononuclear Complexes Supported by 2,4-Dipyrazolyl-6H-1,3,5-triazine and 4,6-Dipyrazolylpyrimidine Ligands
Authors of publication
Capel Berdiell, Izar; Farmiloe, Sarah E.; Kulmaczewski, Rafal; Halcrow, Malcolm
Journal of publication
Dalton Transactions
Year of publication
2019
a
8.0112 ± 0.0002 Å
b
10.5868 ± 0.0003 Å
c
16.9917 ± 0.0003 Å
α
90°
β
95.332 ± 0.002°
γ
90°
Cell volume
1434.88 ± 0.06 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0358
Residual factor for significantly intense reflections
0.0299
Weighted residual factors for significantly intense reflections
0.0756
Weighted residual factors for all reflections included in the refinement
0.08
Goodness-of-fit parameter for all reflections included in the refinement
