Relative hemilabilities of H<sub>2</sub>B(az)<sub>2</sub> (az = pyrazolyl, dimethylpyrazolyl, methimazolyl) chelates in the complexes [M(η-C<sub>3</sub>H<sub>5</sub>)(CO)<sub>2</sub>{H<sub>2</sub>B(az)<sub>2</sub>}] (M = Mo, W).
Authors of publication
Abernethy, Robyn J.; Foreman, Mark R St-J; Hill, Anthony F.; Smith, Matthew K.; Willis, Anthony C.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2020
Journal volume
49
Journal issue
3
Pages of publication
781 - 796
a
7.5475 ± 0.0001 Å
b
18.8361 ± 0.0002 Å
c
14.6355 ± 0.0002 Å
α
90°
β
101.684 ± 0.0005°
γ
90°
Cell volume
2037.55 ± 0.04 Å3
Cell temperature
200 K
Ambient diffraction temperature
200 K
Number of distinct elements
8
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/a 1
Hall space group symbol
-P 2yab
Residual factor for significantly intense reflections
0.0334
Weighted residual factors for all reflections included in the refinement
0.0368
Goodness-of-fit parameter for all reflections included in the refinement
