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Information card for entry 7701896
Preview
Coordinates | 7701896.cif |
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Original paper (by DOI) | HTML |
Formula | C64 H56 B Ni P2 S2 |
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Calculated formula | C64 H56 B Ni P2 S2 |
Title of publication | Reactivity of the diphosphinodithio ligated nickel(0) complex toward alkyl halides and resultant nickel(i) and nickel(ii)-alkyl complexes. |
Authors of publication | Zhang, Ailing; Wang, Congxiao; Lai, Xiaoyu; Zhai, Xiaofang; Pang, Maofu; Tung, Chen-Ho; Wang, Wenguang |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2018 |
Journal volume | 47 |
Journal issue | 44 |
Pages of publication | 15757 - 15764 |
a | 18.6906 ± 0.0003 Å |
b | 21.6675 ± 0.0003 Å |
c | 27.8121 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 11263.3 ± 0.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0513 |
Residual factor for significantly intense reflections | 0.0391 |
Weighted residual factors for significantly intense reflections | 0.0987 |
Weighted residual factors for all reflections included in the refinement | 0.1088 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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