Information card for entry 7701992

Structure parameters

• Formula: C43 H52 Cl2 F3 N2 Ni O3 P S Si
• Calculated formula: C43 H52 Cl2 F3 N2 Ni O3 P S Si
• Title of publication: Neutral, cationic and anionic organonickel and -palladium complexes supported by iminophosphine/phosphinoenaminato ligands.
• Authors of publication: Santiago, Tomás G; Urbaneja, Carmen; Álvarez, Eleuterio; Ávila, Elena; Palma, Pilar; Cámpora, Juan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 2
• Pages of publication: 322 - 335
• a: 10.8549 ± 0.0005 Å
• b: 12.204 ± 0.0006 Å
• c: 18.5076 ± 0.0009 Å
• α: 96.275 ± 0.002°
• β: 94.927 ± 0.002°
• γ: 94.771 ± 0.002°
• Cell volume: 2417.4 ± 0.2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0591
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1171
• Weighted residual factors for all reflections included in the refinement: 0.1268
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No