Crystallography Open Database

Information card for entry 7702074

7702073 << 7702074 >> 7702075

Preview

Coordinates	7702074.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H48 Cl4 Nb P4
Calculated formula	C20 H48 Cl4 Nb P4
Title of publication	Niobium tetrahalide complexes with neutral diphosphine ligands.
Authors of publication	Benjamin, Sophie L.; Chang, Yao-Pang; Hector, Andrew L.; Jura, Marek; Levason, William; Reid, Gillian; Stenning, Gavin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	19
Pages of publication	8192 - 8200
a	10.5571 ± 0.0005 Å
b	11.6652 ± 0.0005 Å
c	11.9053 ± 0.0008 Å
α	90°
β	95.008 ± 0.007°
γ	90°
Cell volume	1460.55 ± 0.14 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.017
Residual factor for significantly intense reflections	0.0166
Weighted residual factors for significantly intense reflections	0.0402
Weighted residual factors for all reflections included in the refinement	0.0404
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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