Information card for entry 7702076

Structure parameters

• Common name: [NbCl4(DMPE)2]
• Formula: C12 H32 Cl4 Nb P4
• Calculated formula: C12 H32 Cl4 Nb P4
• Title of publication: Niobium tetrahalide complexes with neutral diphosphine ligands.
• Authors of publication: Benjamin, Sophie L.; Chang, Yao-Pang; Hector, Andrew L.; Jura, Marek; Levason, William; Reid, Gillian; Stenning, Gavin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 19
• Pages of publication: 8192 - 8200
• a: 10.7216 ± 0.0009 Å
• b: 11.2891 ± 0.001 Å
• c: 9.4711 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1146.36 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0223
• Residual factor for significantly intense reflections: 0.0209
• Weighted residual factors for significantly intense reflections: 0.0453
• Weighted residual factors for all reflections included in the refinement: 0.0457
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No