Information card for entry 7702109

Structure parameters

• Chemical name: [PBr4]2[I5Br7]
• Formula: Br15 I5 P2
• Calculated formula: Br15 I5 P2
• Title of publication: Ionic-liquid-assisted synthesis of the phosphorus interhalides [PBr₄][IBr₂] and [PBr₄][I₅Br₇].
• Authors of publication: Hausmann, David; Köppe, Ralf; Wolf, Silke; Roesky, Peter W.; Feldmann, Claus
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 41
• Pages of publication: 16526 - 16532
• a: 9.2316 ± 0.0018 Å
• b: 9.5736 ± 0.0019 Å
• c: 9.6641 ± 0.0019 Å
• α: 91.12 ± 0.03°
• β: 92.47 ± 0.03°
• γ: 111.88 ± 0.03°
• Cell volume: 791.3 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0575
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1228
• Weighted residual factors for all reflections included in the refinement: 0.1262
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No