Information card for entry 7702118

Structure parameters

• Formula: C14 H30 B18 Co2
• Calculated formula: C14 H30 B18 Co2
• Title of publication: Double deboronation and homometalation of 1,1'-bis(ortho-carborane).
• Authors of publication: Thiripuranathar, Gobika; Chan, Antony P. Y.; Mandal, Dipendu; Man, Wing Y.; Argentari, Mario; Rosair, Georgina M.; Welch, Alan J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 6
• Pages of publication: 1811 - 1821
• a: 7.5433 ± 0.0008 Å
• b: 14.348 ± 0.0012 Å
• c: 21.504 ± 0.0017 Å
• α: 90°
• β: 96.906 ± 0.004°
• γ: 90°
• Cell volume: 2310.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0501
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0748
• Weighted residual factors for all reflections included in the refinement: 0.0784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No