Information card for entry 7702235

Structure parameters

• Formula: C65.922 H70 Co2 N6 O7
• Calculated formula: C65.92 H70 Co2 N6 O7
• Title of publication: Reactions of dicobalt octacarbonyl with dinucleating and mononucleating bis(imino)pyridine ligands.
• Authors of publication: Hollingsworth, Ryan L.; Beattie, Jeffrey W.; Grass, Amanda; Martin, Philip D.; Groysman, Stanislav; Lord, Richard L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 43
• Pages of publication: 15353 - 15363
• a: 19.9171 ± 0.001 Å
• b: 16.047 ± 0.0008 Å
• c: 18.9243 ± 0.0009 Å
• α: 90°
• β: 99.304 ± 0.003°
• γ: 90°
• Cell volume: 5968.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0934
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1454
• Weighted residual factors for all reflections included in the refinement: 0.1668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0506
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No