Crystallography Open Database

Information card for entry 7702260

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Coordinates	7702260.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H35 Fe N2 O P Pd
Calculated formula	C34 H35 Fe N2 O P Pd
Title of publication	Versatile coordination and C-H activation of a multi-donor phosphinoferrocene carboxamide ligand in Pd(ii) complexes.
Authors of publication	Horký, Filip; Škoch, Karel; Císařová, Ivana; Štěpnička, Petr
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	43
Pages of publication	16412 - 16425
a	10.9881 ± 0.0002 Å
b	11.6075 ± 0.0002 Å
c	12.538 ± 0.0003 Å
α	112.701 ± 0.001°
β	95.227 ± 0.001°
γ	97.821 ± 0.001°
Cell volume	1443.39 ± 0.05 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0219
Residual factor for significantly intense reflections	0.0201
Weighted residual factors for significantly intense reflections	0.0478
Weighted residual factors for all reflections included in the refinement	0.0487
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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