Information card for entry 7702288

Structure parameters

• Formula: C40 H32 N8 Ni2 O17 V6
• Calculated formula: C40 H32 N8 Ni2 O17 V6
• Title of publication: Hydrothermal syntheses and crystal structures of two-dimensional (2D) layered vanadium oxide complexes: M(bipy)(H2O)V2O6 (M = Ni, Co, bipy = bipyridine) and [Ni(bipy)2V6O17]
• Authors of publication: Cai-Ming Liu; Song Gao; Huai-Ming Hu; Xianglin Jin; Hui-Zhong Kou
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Pages of publication: 598 - 601
• a: 15.503 ± 0.003 Å
• b: 14.748 ± 0.003 Å
• c: 10.467 ± 0.002 Å
• α: 90°
• β: 92.01 ± 0.03°
• γ: 90°
• Cell volume: 2391.7 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0276
• Weighted residual factors for significantly intense reflections: 0.0613
• Weighted residual factors for all reflections included in the refinement: 0.0692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No