Information card for entry 7702321

Structure parameters

• Formula: C25 H15 N13 O2 Pt3 S8
• Calculated formula: C25 H15 N13 O2 Pt3 S8
• Title of publication: Structural studies of [Pt(CNMe)4][M(mnt)2]n {M = Pd or Pt, mnt = [S2C2(CN)2]2−, n = 1 or 2}: structure-dependent paramagnetism of three crystal forms of [Pt(CNMe)4][Pt(mnt)2]2
• Authors of publication: Bois, Hugues; Connelly, Neil G.; Crossley, John G.; Guillorit, Jean-Christophe; Lewis, Gareth R.; Orpen, A. Guy; Thornton, Peter
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 17
• Pages of publication: 2833
• a: 15.913 ± 0.003 Å
• b: 16.807 ± 0.003 Å
• c: 14.799 ± 0.003 Å
• α: 90°
• β: 96.417 ± 0.003°
• γ: 90°
• Cell volume: 3933.2 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0917
• Residual factor for significantly intense reflections: 0.0677
• Weighted residual factors for all reflections: 0.1755
• Weighted residual factors for significantly intense reflections: 0.1542
• Goodness-of-fit parameter for all reflections: 1.262
• Goodness-of-fit parameter for significantly intense reflections: 1.294
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No