Information card for entry 7702357

Structure parameters

• Formula: C82 H106 Cu4 F24 N26 O10 P4
• Calculated formula: C82 H106 Cu4 F24 N26 O10 P4
• Title of publication: Tetranuclear grid-like copper(II) complexes with pyrazolate bridges: syntheses, structures, magnetic and EPR spectroscopic properties
• Authors of publication: Mann, Karen L. V.; Psillakis, Elefteria; Jeffery, John C.; Rees, Leigh H.; Harden, Nicholas M.; McCleverty, Jon A.; Ward, Michael D.; Gatteschi, Dante; Totti, Federico; Mabbs,, Frank E.; McInnes, Eric J. L.; Riedi, Peter C.; Smith, Graham M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 3
• Pages of publication: 339
• a: 19.567 ± 0.002 Å
• b: 26.313 ± 0.003 Å
• c: 20.033 ± 0.003 Å
• α: 90°
• β: 91.441 ± 0.01°
• γ: 90°
• Cell volume: 10311 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1739
• Residual factor for significantly intense reflections: 0.0792
• Weighted residual factors for all reflections: 0.2
• Weighted residual factors for significantly intense reflections: 0.1606
• Goodness-of-fit parameter for all reflections: 1.04
• Goodness-of-fit parameter for significantly intense reflections: 1.214
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No