Crystallography Open Database

Information card for entry 7702359

Preview

Coordinates	7702359.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[La(tbpa)(H2O)(m-ClO4)] (ClO4)2.2CHCl3.MeOH
Formula	C36 H35 Cl9 La N7 O14
Calculated formula	C36 H27 Cl9 La N7 O14
Title of publication	A rare uranium(III) complex of a tripodal aromatic amine and its lanthanum analogue
Authors of publication	Wietzke, Raphaël; Mazzanti, Marinella; Latour, Jean-Marc; Pécaut, Jacques
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1998
Journal issue	24
Pages of publication	4087
a	11.9085 ± 0.0001 Å
b	13.3371 ± 0.0002 Å
c	18.2306 ± 0.0003 Å
α	69.647 ± 0.001°
β	87.536 ± 0.001°
γ	64.078 ± 0.001°
Cell volume	2421.07 ± 0.07 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.038
Residual factor for significantly intense reflections	0.0341
Weighted residual factors for significantly intense reflections	0.0872
Weighted residual factors for all reflections included in the refinement	0.0895
Goodness-of-fit parameter for all reflections included in the refinement	1.082
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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