Information card for entry 7702371

Structure parameters

• Common name: bis-tripicolylaminecalcium perchlorate
• Chemical name: bis-tri(2-pyridylmethyl)aminecalcium diperchlorate
• Formula: C36 H36 Ca Cl2 N8 O8
• Calculated formula: C36 H36 Ca0.5 Cl2 N8 O8
• Title of publication: Synthesis and structural characterisation of Group I and II metal complexes involving the ligand tris(2-pyridylmethyl)amine
• Authors of publication: Hazell, Alan; McGinley, John; Toftlund, Hans
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 8
• Pages of publication: 1271
• a: 9.7069 ± 0.0005 Å
• b: 10.8978 ± 0.0005 Å
• c: 18.3622 ± 0.0009 Å
• α: 90°
• β: 103.411 ± 0.001°
• γ: 90°
• Cell volume: 1889.46 ± 0.16 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.051
• Goodness-of-fit parameter for significantly intense reflections: 1.757
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No