Information card for entry 7702393

Structure parameters

• Formula: C22 H56 I10 N4 Pb3
• Calculated formula: C22 H56 I10 N4 Pb3
• Title of publication: Discrete and polymeric iodoplumbates with Pb3I10 building blocks: [Pb3I10]4−, [Pb7I22]8−, [Pb10I28]8−, 1\ιnfty [Pb3I10]4− and 2∞[Pb7I18]4−
• Authors of publication: Krautscheid, Harald; Vielsack, Frieder
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 16
• Pages of publication: 2731
• a: 20.889 ± 0.002 Å
• b: 13.2764 ± 0.001 Å
• c: 18.4226 ± 0.0017 Å
• α: 90°
• β: 101.245 ± 0.01°
• γ: 90°
• Cell volume: 5011.1 ± 0.8 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0626
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1334
• Weighted residual factors for all reflections included in the refinement: 0.1378
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No