Information card for entry 7702400

Structure parameters

• Formula: C86 H92 Cl4 O18 P4 Re4
• Calculated formula: C86 H92 Cl4 O18 P4 Re8
• Title of publication: The first symmetrical tetrarheniumcyclodiyne type cluster containing phosphine ligands: Re4(μ-O)4Cl4[P(C6H4OMe-p)3]4
• Authors of publication: Lau, Sophia S.; Fanwick, Phillip E.; Walton, Richard A.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 14
• Pages of publication: 2273
• a: 13.9995 ± 0.0007 Å
• b: 23.5126 ± 0.0007 Å
• c: 14.3633 ± 0.0007 Å
• α: 90°
• β: 114.2 ± 0.0016°
• γ: 90°
• Cell volume: 4312.4 ± 0.3 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.062
• Weighted residual factors for all reflections included in the refinement: 0.104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.138
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No