Information card for entry 7702426

Structure parameters

• Formula: C29.5 H69 Li3 N12 Si6
• Calculated formula: C29.5 H63 Li3 N12 Si6
• Title of publication: Reactions of 1,3,5-triazine with organolithium compounds containing trimethylsilyl substituents; X-ray structures of 1,3,5-triaza- and 1,3,5,7-tetraaza-heptatrienyllithium compounds †
• Authors of publication: Boesveld, W. Marco; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 22
• Pages of publication: 4041
• a: 18.869 ± 0.007 Å
• b: 14.603 ± 0.004 Å
• c: 19.523 ± 0.004 Å
• α: 90°
• β: 112.1 ± 0.02°
• γ: 90°
• Cell volume: 4984 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1186
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for all reflections: 0.1608
• Weighted residual factors for significantly intense reflections: 0.1316
• Goodness-of-fit parameter for all reflections: 1.02
• Goodness-of-fit parameter for significantly intense reflections: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No