Information card for entry 7702545

Structure parameters

• Formula: C33 H31 B2 Eu N12 O2
• Calculated formula: C33 H31 B2 Eu N12 O2
• Title of publication: Structural studies of some mono- and bi-nuclear heteroleptic trispyrazolyborate complexes containing eight-co-oordinated europium and gadolinium†
• Authors of publication: Lawrence, Royston G.; Hamor, Thomas A.; Jones, Christopher J.; Paxton, Keith; Rowley, Natalie M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 14
• Pages of publication: 2121
• a: 16.994 ± 0.005 Å
• b: 11.179 ± 0.004 Å
• c: 18.466 ± 0.007 Å
• α: 90°
• β: 90.24 ± 0.01°
• γ: 90°
• Cell volume: 3508 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0194
• Residual factor for significantly intense reflections: 0.0185
• Weighted residual factors for all reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.0459
• Goodness-of-fit parameter for all reflections: 1.081
• Goodness-of-fit parameter for significantly intense reflections: 1.086
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No