Information card for entry 7702548

Structure parameters

• Formula: C48 H52 B4 Cl8 Gd2 N24 O4
• Calculated formula: C48 H52 B4 Cl8 Gd2 N24 O4
• Title of publication: Structural studies of some mono- and bi-nuclear heteroleptic trispyrazolyborate complexes containing eight-co-oordinated europium and gadolinium†
• Authors of publication: Lawrence, Royston G.; Hamor, Thomas A.; Jones, Christopher J.; Paxton, Keith; Rowley, Natalie M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 14
• Pages of publication: 2121
• a: 11.676 ± 0.002 Å
• b: 16.091 ± 0.004 Å
• c: 18.162 ± 0.004 Å
• α: 90°
• β: 97.51 ± 0.01°
• γ: 90°
• Cell volume: 3383 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0909
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for all reflections: 0.1729
• Weighted residual factors for significantly intense reflections: 0.1549
• Goodness-of-fit parameter for all reflections: 1.063
• Goodness-of-fit parameter for significantly intense reflections: 1.088
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No